A study of the effects of sintering time variation on the superconducting properties of a Pb-doped BSCCO superconductor prepared by second combustion method

Date of Publication

1995

Document Type

Bachelor's Thesis

Degree Name

Bachelor of Science Major in Physics

Subject Categories

Physics

College

College of Science

Department/Unit

Physics

Abstract/Summary

The effects of the sintering time variation on the superconducting properties of a Pb-doped BSCCO superconductor was determined. The samples were prepared using the second combustion method. X-ray diffractrometry and R-T tests were used to characterize the bulk samples. Using the LSUCR-87 program, a tetragonal crystal structure was obtained for all the samples. For the low-Tc phase, the average crystallographic constants obtained are a = 5.37879 A and C = 30.98261 A. For the high-Tc phase, the average crystallographic constants obtained are a = 5.40713 A and C = 37.35328 A. These values are comparable to those obtained by Koyama 29 (a = 5.3960 A and c = 37.1800 A) and Maeda (a = 5.4130 A and c = 37.1000 A). The sample sintered for 30 hours has the highest percentage of high-Tc peaks. This is consistent with the R-T characterization results where the critical temperature is 103K.

Abstract Format

html

Language

English

Format

Print

Accession Number

TU06729

Shelf Location

Archives, The Learning Commons, 12F, Henry Sy Sr. Hall

Physical Description

57 leaves ; Computer print-out.

Keywords

Superconductors--Magnetic properties; Sintering; Electric conductivity; Combustion; Lead

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