An investigation on recovery techniques for citric acid and acetic acid: A project study

Date of Publication

1990

Document Type

Bachelor's Thesis

Degree Name

Bachelor of Science in Chemical Engineering

Subject Categories

Chemical Engineering

College

Gokongwei College of Engineering

Department/Unit

Chemical Engineering

Honor/Award

Awarded as best thesis, 1990

Thesis Adviser

Luz G. Paca

Abstract/Summary

Techniques of the recovery of citric acid and acetic acid from fermentation broth using conventional methods were investigated. Operations of two critical steps in citric acid recovery, liming and acidulation were optimized. It was found out that 25% lime at 50C gave the best result for a constant citric acid concentration in feed of 10.81 % W. For acidulation, 15% H2SO4 gave the maximum percent conversion of 94.74 %. For acetic acid recovery, a maximum of 50% W acetic acid was obtained after solvent extraction. The effect of azeotropic distillation was a further increase of concentration to at most 97% W acetic acid.

Abstract Format

html

Language

English

Format

Print

Accession Number

TU04710

Shelf Location

Archives, The Learning Commons, 12F Henry Sy Sr. Hall

Physical Description

xiii, 125 leaves : ill. ; 28 cm.

Keywords

Citric acid; Acetic acid

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